Description
The D8 ADVANCE X-ray diffractometer is one of the most powerful and versatile instruments for characterizing the crystallinity of natural and synthetic materials.
Year of manufacture 2009. Serviced by Bruker on 2/12/2020.
The diffractometer software allows you to perform SAXS (Small Angle X-ray Scattering) and WAXS (Wide Angle X-ray Scattering) measurements. You can change the angular range and acquisition mode by changing the integration time and the angular step.
Main technical specifications:
Configuration: 𝜃/𝜃 or 𝜃/2𝜃
Default measurement diameter: 500 mm and 560 mm
Angular range: 360°
Measurable range: −110° < 2𝜃 ≤ 168°
Angular resolution: 0.0001°
Maximum angular velocity: 20°/s
Regarding other analyses:
✔ SAXS/WAXS measurements → Yes, supported by the diffractometer software.
✔ PDF Analysis → Possible via Xpowder, but not with the native software of the diffractometer (DIFFRAC.EVA, license expired). However, the installed software has a PDF2 Powder Diffraction File database (2010) for phase identification.
✖ Rietveld Analysis (TOPAS) → Not supported by the native software. Alternative software, from Bruker or third parties, must be obtained.
Important note:
The powder sample for XRD analysis does not rotate during measurements. If rotation is necessary to improve the statistics of the measurements, an alternative solution must be found, such as the use of a rotating sample holder compatible with the system.
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